Volume 34 Issue 4
Jul.  2017
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QU Jianfeng, QIU Zhengsong, GUO Baoyu, ZHONG Hanyi, WANG Weiji, MAO Hui. Synthesis and Evaluation of a New Graphene Oxide High Temperature Filter Loss Reducer[J]. DRILLING FLUID & COMPLETION FLUID, 2017, 34(4): 9-14. doi: 10.3969/j.issn.1001-5620.2017.04.002
Citation: QU Jianfeng, QIU Zhengsong, GUO Baoyu, ZHONG Hanyi, WANG Weiji, MAO Hui. Synthesis and Evaluation of a New Graphene Oxide High Temperature Filter Loss Reducer[J]. DRILLING FLUID & COMPLETION FLUID, 2017, 34(4): 9-14. doi: 10.3969/j.issn.1001-5620.2017.04.002

Synthesis and Evaluation of a New Graphene Oxide High Temperature Filter Loss Reducer

doi: 10.3969/j.issn.1001-5620.2017.04.002
  • Received Date: 2017-05-17
  • Publish Date: 2017-07-31
  • A GO/polymer filter loss reducer GOJ was made through copolymerization of graphene oxide (GO), acrylamide (AM), 2-Acrylamido-2-methylpropane sulfonic acid (AMPS), dimethyl diallyl ammonium chloride (DMDAAC) and vinyl acetate (VAC). Characterization of the synthesized product with IR and TEM photography showed that there are pentacyclic structure and amide group, sulfonic group, hydroxyl group in the GOJ molecules. GOJ has relative molecular weight of about 3.63×105. Observed under the microscope, GOJ has dark color and a levelling platy structure. Drilling fluid laboratory experiment showed that GOJ has good filtration control property. A fresh water base drilling fluid treated with 0.2% GOJ has its API filter loss reduced by 70%, indicating that the performance of GOJ is better than PAMS601 and JT888. GOJ has good salt resistant, and can be used in saturated salt drilling fluid. At the same concentration in drilling fluid, the filtration rates of the drilling fluids treated with GOJ under 180℃, 200℃ and 220℃ are all lower than that of the drilling fluids treated with Driscal-D under the same temperature, respectively. Graphene oxide has the ability to enhance the temperature resistance of GOJ; when GOJ contains 0.32% graphene oxide, the temperature resistance of GOJ is increased by about 20℃, and with the increase of the content of graphene oxide in GOJ, the high temperature filtration control performance of GOJ is also increased.

     

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