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聚胺抑制剂的测定方法及最佳用量的确定

郭建华,  马文英,  刘晓燕,  杜明军,  李保慧,  钟灵

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文章导航 > 钻井液与完井液  > 2016 >  33(3): 35-40
郭建华, 马文英, 刘晓燕, 杜明军, 李保慧, 钟灵. 聚胺抑制剂的测定方法及最佳用量的确定[J]. 钻井液与完井液, 2016, 33(3): 35-40. doi: 10.3969/j.issn.1001-5620.2016.03.007
引用本文: 郭建华, 马文英, 刘晓燕, 杜明军, 李保慧, 钟灵. 聚胺抑制剂的测定方法及最佳用量的确定[J]. 钻井液与完井液, 2016, 33(3): 35-40. doi: 10.3969/j.issn.1001-5620.2016.03.007
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GUO Jianhua, MA Wenying, LIU Xiaoyan, DU Mingjun, LI Baohui, ZHONG Ling. Ploya mine Shale Inhibitor Content Measurement and Determination of Optimum Dosage[J]. DRILLING FLUID & COMPLETION FLUID, 2016, 33(3): 35-40. doi: 10.3969/j.issn.1001-5620.2016.03.007
Citation: GUO Jianhua, MA Wenying, LIU Xiaoyan, DU Mingjun, LI Baohui, ZHONG Ling. Ploya mine Shale Inhibitor Content Measurement and Determination of Optimum Dosage[J]. DRILLING FLUID & COMPLETION FLUID, 2016, 33(3): 35-40. doi: 10.3969/j.issn.1001-5620.2016.03.007
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聚胺抑制剂的测定方法及最佳用量的确定

doi: 10.3969/j.issn.1001-5620.2016.03.007
  • 1.

    中石化中原石油工程有限公司钻井工程技术研究院, 河南濮阳 457001

  • 2. 中石化中原石油工程有限公司钻井二公司, 河南濮阳 457001

基金项目: 中石化部级项目“高效聚胺抑制剂在油气井水平段钻井应用试验”（J214001）。
详细信息
    作者简介:

    郭建华,男,高级工程师,硕士研究生,1970年生,1996年毕业于西南石油学院应用化学专业,现在主要从事管理、钻井液及防漏堵漏技术研究工作。电话(0393)4899234;E-mail:zyzjygjh@163.com。

  • 中图分类号: TE254.4

Ploya mine Shale Inhibitor Content Measurement and Determination of Optimum Dosage

  • 1.

    Research Center of Engineering Technology, Zhongyuan Engineering Company, Puyang, Henan 457001

  • 2. No. 2 Drilling Department of Zhongyuan Engineering Company, Puyang, Henan 457001

    摘要
  • 摘要: 目前，聚胺作为一种水基钻井液用高效抑制剂得到广泛应用，但对它的研究还主要集中在抑制性评价和现场应用效果中。为此探索研究了聚胺抑制剂含量的测定方法，采用四苯硼钠法进行游离聚胺（FYZ-1）含量测定，通过对指示剂、沉淀条件、滴定条件、pH值调节剂等实验条件的优化，确定了测定方法，并进行岩屑对聚胺含量影响实验。结果表明，碳质泥岩、易水化泥岩、硬脆性泥岩、砂岩对聚胺吸附依次降低，据此可以推荐聚胺在不同地层的加量并指导现场应用。

     

    Abstract: As a high performance shale inhibitor, polyamine has found a wide application in drilling with water base drilling fluids. Studies on polyamine were primarily focused on the inhibitive capacity and field application, and no technical specifications of polyamine have been established. A method of measuring the content of polyamine is discussed in this paper. Using the "sodium tetraphenylborate method", the content of a free polyamine, FYZ-1, was measured. The measuring method has been determined through the optimization of the testing conditions, such as indicators, precipitation conditions, titration conditions, pH values, etc. The effect of drill cuttings on the content of polyamine has also been studied. It has been founded in laboratory experiments that the quantities of the adsorbed polyamine on carbonaceous shale, hydratable shale, brittle shale and sandstone are decreasing in that order. This finding can be used to determine the concentrations of polyamine in drilling fluids in field operations.

     

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出版历程
  • 收稿日期:  2016-01-05
  • 刊出日期:  2016-05-31

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