Volume 36 Issue 1
Feb.  2019
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LIU Haoya, BAO Hongzhi, ZHAO Wei. Study on Microscopic Hydration Process of a Cold Temperature Cement Slurry Used in Frozen Areas at -18 ℃[J]. DRILLING FLUID & COMPLETION FLUID, 2019, 36(1): 77-81. doi: 10.3969/j.issn.1001-5620.2019.01.015
Citation: LIU Haoya, BAO Hongzhi, ZHAO Wei. Study on Microscopic Hydration Process of a Cold Temperature Cement Slurry Used in Frozen Areas at -18 ℃[J]. DRILLING FLUID & COMPLETION FLUID, 2019, 36(1): 77-81. doi: 10.3969/j.issn.1001-5620.2019.01.015

Study on Microscopic Hydration Process of a Cold Temperature Cement Slurry Used in Frozen Areas at -18 ℃

doi: 10.3969/j.issn.1001-5620.2019.01.015
  • Received Date: 2018-12-05
  • Publish Date: 2019-02-28
  • The cold sea area in polar region of the earth possess huge reserves of oil and gas, cementing of the wells developing these oil and gas is not able to be completed using conventional cement slurries because the water in the cement slurry gets frozen in cold temperatures in polar region, and the hydration of cement is unable to proceed. A cement slurry has recently been developed for use in this cold area, and the products of hydration at -18 ℃ and at room temperature were compared microscopically. Laboratory experimental results showed that the cement slurry developed has excellent setting performance at cold temperatures; at -18 ℃, the cement slurry sets in 0.5-3 h, and the 24 h compressive strength falls between 3.5 and 9 MPa, indicating that the cement slurry can be used to resolve the problems conventional cement slurries have to face with: being unable to set and having no strength at cold temperatures. Microscopic test of the cement slurry shoed that the hydration degree of the cement slurry at -18 ℃ is lower than that of the cement slurry at room temperature, while the Aft content of the cement slurry at -18 ℃ is higher than that of the cement slurry at room temperature, a phenomenon that is positive to the mechanical properties of the set cement.

     

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  • [1]
    魏鹏. 不同温度下水化硅酸钙复合材料力学性能的分子动力学研究[D]. 深圳:深圳大学,2017.12-35 WEI Peng. Molecular dynamics study of mechanical properties of calcium silicate composites at different temperatures[D]. Shenzhen:Shenzhen University, 2017.12

    -35.
    [2]
    王瑞和,王成文,步玉环,等.深水固井技术研究进展[J]. 中国石油大学学报,2008, 32(1):77-81.

    WANG Ruihe, Chengwen, BU Yuhuan,et al. Research development of deepwaterTechnique[J]. Journal of China University of Petroleum,2008,32(1):77-81.
    [3]
    И И Белей,Л М Каргапольцева. Новый порошкообразный расширяющийся тампонажный материал для низких температур[J]. Троительство нефтяных и газовых скважин на суше и на море,2007(в):33-37.
    [4]
    LOTHEN BACH B,MATSCHEI T,MOSCHNER G,et al. Thermody-namic modeling of the effect of temperature on the hydration and porosity of Portland cement[J]. Cem Concr Res,2008,38(1):1-8.
    [5]
    ESCALANTE-GARCIA J I,SHARP J H. Variation in the composition of C-S-H gel in Portland cement pastes cured at various temperatures[J]. J Am Ceram Soc,1999,82(11):3237-3243.
    [6]
    THOMAS J J,ROTHSTEIN D,JENNINGS H M,et al. Effect of hydration temperature on the solubility behavior of Ca-,S-,Al-,and Si-bearing solid phases in Portland cement pastes[J].Cem Concr Res,2003,33(12):2037-2042.
    [7]
    徐玲琳,李楠,王培铭,等. 温度对铝酸盐水泥基三元体系早期水化的影响[J]. 硅酸盐学报,2016,44(11):1152-1157.

    XU Lingl in,LI Nan,WANG,et al.Pe iming temperature effect on early hydration of calcium aluminate cement based ternary blends[J].Journal of The Chinese Ceramic Society,2016,44(11):1152-1157.
    [8]
    WINNEFELD F,LOTHENBACH B.Hydration of calcium sulfoaluminate cements-experimental findings and thermodynamic modelling[J].Cem Concr Res,2010, 40(8):1239-1247.
    [9]
    KWANS,LAROSAJ,GRUTZECKMW. 29Si and 27AlMASNMR study of stratlingite[J]. J Am Ceram Soc, 1995,78(7):1921-1926.
    [10]
    王培铭,徐冷琳,张国防.0-20℃养护下硅酸盐水泥水化时钙矾石的生成及转变[J]. 硅酸盐学报,2012, 40(5):646-650.

    WANG Peiming,XU Linglin,ZHANG Guofang. Formation and conversion of ettringite during hydration of portland cement from 0 to 20℃[J]. Journal of the Chinese Ceramic Society,2012,40(5):646-650.
    [11]
    王玉锁,叶跃忠,钟新樵,等. 新型混凝土早强剂的应用研究现状[J]. 建筑材料,2005(4):105-106. WANG Yusuo,YE Yuezhong,ZHONG Xinyu,et al. Application status of new concrete early strength agent[J]. Building Materials,2005

    (4):105-106.
    [12]
    邓君安,李德栋,李启棣,等. 硫铝酸盐早强水泥负温下的水化硬化[J]. 硅酸盐学报,1983(11):85-94. DENG Junan,LI DEdong,LI Qikai,et al. The hydration and hardening of high early strength sulfoaluminate cement under subzero performance[J]. Journal of the Chinese Ceramic Society,1983

    (11):85-94.
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