Volume 34 Issue 4
Jul.  2017
Turn off MathJax
Article Contents
QU Jianfeng, QIU Zhengsong, GUO Baoyu, ZHONG Hanyi, WANG Weiji, MAO Hui. Synthesis and Evaluation of a New Graphene Oxide High Temperature Filter Loss Reducer[J]. DRILLING FLUID & COMPLETION FLUID, 2017, 34(4): 9-14. doi: 10.3969/j.issn.1001-5620.2017.04.002
Citation: QU Jianfeng, QIU Zhengsong, GUO Baoyu, ZHONG Hanyi, WANG Weiji, MAO Hui. Synthesis and Evaluation of a New Graphene Oxide High Temperature Filter Loss Reducer[J]. DRILLING FLUID & COMPLETION FLUID, 2017, 34(4): 9-14. doi: 10.3969/j.issn.1001-5620.2017.04.002

Synthesis and Evaluation of a New Graphene Oxide High Temperature Filter Loss Reducer

doi: 10.3969/j.issn.1001-5620.2017.04.002
  • Received Date: 2017-05-17
  • Publish Date: 2017-07-31
  • A GO/polymer filter loss reducer GOJ was made through copolymerization of graphene oxide (GO), acrylamide (AM), 2-Acrylamido-2-methylpropane sulfonic acid (AMPS), dimethyl diallyl ammonium chloride (DMDAAC) and vinyl acetate (VAC). Characterization of the synthesized product with IR and TEM photography showed that there are pentacyclic structure and amide group, sulfonic group, hydroxyl group in the GOJ molecules. GOJ has relative molecular weight of about 3.63×105. Observed under the microscope, GOJ has dark color and a levelling platy structure. Drilling fluid laboratory experiment showed that GOJ has good filtration control property. A fresh water base drilling fluid treated with 0.2% GOJ has its API filter loss reduced by 70%, indicating that the performance of GOJ is better than PAMS601 and JT888. GOJ has good salt resistant, and can be used in saturated salt drilling fluid. At the same concentration in drilling fluid, the filtration rates of the drilling fluids treated with GOJ under 180℃, 200℃ and 220℃ are all lower than that of the drilling fluids treated with Driscal-D under the same temperature, respectively. Graphene oxide has the ability to enhance the temperature resistance of GOJ; when GOJ contains 0.32% graphene oxide, the temperature resistance of GOJ is increased by about 20℃, and with the increase of the content of graphene oxide in GOJ, the high temperature filtration control performance of GOJ is also increased.

     

  • loading
  • [1]
    马喜平,周有祯,韩国彤. 一种钻井液降滤失剂的合成与室内评价[J].精细化工, 2015, 32(7):799-805.

    MA Xiping, ZHOU Youzhen, HAN Guotong, et al. Synthesis and indoor evaluation of a fluid loss additive with significant inhibition effect[J]. Fine Chemicals, 2015, 32(7):799-805.
    [2]
    柏嵩,沈小平. 石墨烯基无机纳米复合材料[J]. 化学进展, 2010, 22(11):2106-2118.

    BAI Song, SHEN Xiaoping. Graphene-based inorganic nanocomposites[J].Progress In Chemistry, 2010, 22(11):2106-2118.
    [3]
    王彦. 石墨烯的制备及其在聚合物复合材料中的应用[D]. 上海:上海交通大学, 2012. WANG Yan. Synthesis of grapheme and its application in polymer composites[D]. Shanghai:Shanghai Jiao Tong University,2012.
    [4]
    陈朝然. 纳米改性钻井液及对铝合金钻杆减摩性能研究[D]. 吉林:吉林大学, 2016. CHEN Zhaoran. Effect of nano particles addition on drilling fluid properties and anti friction performance to aluminum alloy drill pipe[D]. Jilin:Jilin University,2016.
    [5]
    许园. 基于改性氧化石墨烯作为低渗透油藏注水开发纳米减阻剂研究[D]. 成都:西南石油大学,2015. XU Yuan. Study based on modified grapheme oxide as nano-drag reduction in low permeability reservoir water flooding[D].Chengdu:Southwest petroleum university, 2015.
    [6]
    孟祖超, 李谦定, 李善建,等. 新型油田污水除油剂的制备及性能研究[J]. 工业水处理, 2016, 36(4):33-36.

    MENG Zuchao, LI Qianding,LI Shanjian, et al. Research on the synthesis and performances of a new type of oil removing agent used for treating oilfield wastewater[J]. Industrial Water Treatment,2016, 36(4):33-36.
    [7]
    MONTEIRO O, QUINTERO L. Graphene-containing fluids for oil and gas exploration and production:U.S. Patent Application 13/424,549[P]. 2012-3-20.
    [8]
    TOUR J M, SCHMIDT H K, LOMEDA J R, et al. Graphene compositions and drilling fluids derived therefrom:U.S. Patent 8,183,180[P]. 2012-5-22.
    [9]
    AFTAB A, ISMAIL A R, IBUPOTO Z H. Enhancing the rheological properties and shale inhibition behavior of water-based mud using nanosilica, multi-walled carbon nanotube, and graphene nanoplatelet[J]. Egyptian journal of petroleum, 2017, 26(2):291-299.
    [10]
    NGUYEN B D, NGO T K, BUI T H, et al. The impact of graphene oxide particles on viscosity stabilization for diluted polymer solutions using in enhanced oil recovery at HTHP offshore reservoirs[J]. Advances in Natural Sciences:Nanoscience and Nanotechnology, 2014, 6(1):015012.
    [11]
    CHAI Y H, YUSUP S, CHOK V S. A review on nanoparticle addition in base fluid for improvement of biodegradable ester-based drilling fluid properties[J]. Chemical Engineering, 2015, 45.
    [12]
    SRIDHARAN V, RAJA T, MUTHUKRISHNAN N. Study of the effect of matrix, fibre treatment and graphene on delamination by drilling jute/epoxy nanohybrid composite[J]. Arabian Journal for Science and Engineering, 2016, 41(5):1883-1894.
    [13]
    HUANG W, WU Y, QIU L, et al. Tuning rheological performance of silica concentrated shear thickening fluid by using graphene oxide[J]. Advances in Condensed Matter Physics, 2015.
    [14]
    HOELSCHER K P, YOUNG S, FRIEDHEIM J, et al. Nanotechnology application in drilling fluids[C]//Offshore Mediterranean Conference and Exhibition. Offshore Mediterranean Conference, 2013.
    [15]
    JAMES D K, TOUR J M. Graphene:Powder, flakes, ribbons, and sheets[J]. Accounts of chemical research, 2012, 46(10):2307-2318.
    [16]
    宣扬,蒋官澄,黎凌,等.高性能纳米降滤失剂氧化石墨烯的研制与评价[J].石油学报,2013,34(5):1010-1016.

    XUAN Yang,JIANG Guancheng,LI Ling,et al.Preparation and evaluation of nano-graphene oxide as a high-performance fluid loss additive[J].Acta Petrolei Sinica,2013,34(5):1010-1016.
    [17]
    TAHA N M, LEE S. Nano graphene application improving drilling fluids performance[C]//International Petroleum Technology Conference. International Petroleum Technology Conference, 2015.
    [18]
    KOSYNKIN D V, CERIOTTI G, WILSON K C, et al. Graphene oxide as a high-performance fluid-loss-control additive in water-based drilling fluids[J]. ACS Applied Materials & Interfaces, 2011, 4(1):222-227.
    [19]
    高党国, 马宇娟. 氧化石墨烯与聚羧酸减水剂单体共聚物的制备与性能[J]. 精细化工, 2015, 32(1):103-107.

    GAO Dangguo, MA Yujuan. Preparation and properties of copolymer of graphene oxide and monomers of polycarboxylate superplasticizer[J]. Fine Chemicals, 2015, 32(1):103-107.
    [20]
    PAREDES J I, VILLAR-RODIL S, MARTÍNEZALONSO A, et al. Graphene oxide dispersions in organic solvents[J]. Langmuir, 2008, 24(19):10560-10564.
    [21]
    周瀚. 聚合物型水基成膜降失水剂的合成与研究[D]. 成都:西南石油大学, 2011. ZHOU Han. Synthesis and study of polymer membrane filtration control agent[D].Chengdu:Southwest petroleum university, 2011.
    [22]
    黄维安.超深井钻井液高温稳定机理与应用研究[D]. 青岛:中国石油大学(华东),2007. HUANG Weian. Study on high-temperature stabilization mechanisms and application of ultra-deep well drilling fluid[D].Qingdao:China university of petroleum(East China),2007.
    [23]
    XU L Q, LIU Y L, NEOH K G, et al. Reduction of graphene oxide by aniline with its concomitant oxidative polymerization[J]. Macromolecular rapid communications, 2011, 32(8):684-688.
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Article Metrics

    Article views (678) PDF downloads(223) Cited by()
    Proportional views
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return