Volume 34 Issue 2
Mar.  2017
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JIANG Guancheng, QI Yourong, AN Yuxiu, GE Qingying, ZHANG Lingyu. Synthesis and Evaluation of a High Temperature AMPS/AM/NVP Copolymer Filter Loss Reducer[J]. DRILLING FLUID & COMPLETION FLUID, 2017, 34(2): 39-44. doi: 10.3969/j.issn.1001-5620.2017.02.007
Citation: JIANG Guancheng, QI Yourong, AN Yuxiu, GE Qingying, ZHANG Lingyu. Synthesis and Evaluation of a High Temperature AMPS/AM/NVP Copolymer Filter Loss Reducer[J]. DRILLING FLUID & COMPLETION FLUID, 2017, 34(2): 39-44. doi: 10.3969/j.issn.1001-5620.2017.02.007

Synthesis and Evaluation of a High Temperature AMPS/AM/NVP Copolymer Filter Loss Reducer

doi: 10.3969/j.issn.1001-5620.2017.02.007
  • Received Date: 2016-12-05
  • Publish Date: 2017-03-31
  • Filter loss reducers presently in use had poor stability and filtration control ability in drilling deep and ultra-deep wells. To overcome these problems, a terpolymer filter loss reducer has been synthesized in laboratory with 2-acrylamido-2-methylpropane sulfonic acid (AMPS), acrylamide (AM), and N-vinyl pyrrolidone (NVP). The optimum synthesis conditions were as follows:molar ratio of AM:AMPS:NVP=6:3:1, concentration of initiator=0.2%, concentrations of the monomers used was 1.5%, respectively, reaction temperature=50℃, and the reaction time=4 h. Structure analysis of the synthesized product with IR spectroscopy showed that it was a terpolymer, and TEM analysis showed that the synthesized product formed an ordered space network structure in water solution. In a 4% fresh water base drilling fluid, the high temperature stability of the synthesized filter loss reducer was remarkably better than that of PAC-LV; the synthesized filter loss reducer functioned effectively at 180℃.

     

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  • [1]
    SPOONER M,MAGEE K,OTTO M,et al.The application of HTHP water based drilling fluid on a blowout operation[C]//The AADE 2003 National Technology Conference.Houston,April 1-3,2003.
    [2]
    BILLY G C,CHARLES P,GEORGE W B.Drilling fluid systems with improved fluid loss properties:US, 7439209[P].2008-10-21.
    [3]
    王中华.AMPS/AM/AN三元共聚物降滤失剂的合成与性能[J]. 油田化学,1995,12(4):367-369.

    WANG Zhonghua.Synthesis and properties of AMPS/AM/AN terpolymer as filterate loss controller for drilling fluids[J].Oilfield Chemistry,1995,12(4):367-369.
    [4]
    王中华. 超高温钻井液降滤失剂P(AMPS-AM-AA)/SMP的研制[J]. 石油钻探技术,2010,5(3):8-12.

    WANG Zhonghua. Development of the P(AMPS-AMAA)/SMP filtration agent used for ultra-high temperature drilling fluid[J].Petroleum Drilling Techniques,2010,5(3):8-12.
    [5]
    王中华,王旭. 超高温钻井液体系研究(Ⅲ)——抗盐高温高压降滤失剂研制[J]. 石油钻探技术,2009, 37(5):5-9.

    WANG Zhonghua, WANG Xu. Studies on ultra-high temperature drilling fluid system(Ⅲ) -development of the salt-resistant high temperature and high pressure fluid loss reagen[J]. Petroleum Drilling Techniques, 2009,37(5):5-9.
    [6]
    谭春勤, 徐江, 孙文俊, 等. 深井油井水泥耐盐抗温降失水剂JSS300的试验研究[J]. 石油钻探技术,2009, 37(4):50-53.

    TAN Chunqin,XU Jiang,SUN Wenjun,et al. JSS300:a high temperature and salt resistant fluid loss agent for deep well cement slurry[J]. Petroleum Drilling Techniques,2009,37(4):50-53.
    [7]
    朱兵, 聂育志, 邱在磊, 等. AMPS/DAMA/AA共聚物固井降滤失剂的研究[J]. 石油钻探技术, 2014, 42(6):40-44.

    ZHU Bing,NIE Yuzhi,QIU Zailei et al. Research on fluid loss additives of AMPS/DMAM/AA in well cementing[J]. Petroleum Drilling Techniques,2014,42(6):40-44.
    [8]
    于永金, 卢海川, 靳建洲, 等. 抗高温降失水剂AMPS/AM/NVP共聚物的合成及性能[J]. 精细石油化工进展, 2010, 11(12):6-8.

    YU Yongjin,LU Haichuan,JIN Jianzhou,et al. Synthesis and performance of thermostable AMPS/AM/NVP copolymer fluid loss additive[J].Andvance in fine Petrochemicals,2010,11(12):6-8.
    [9]
    高磊,孙德军,徐建. 聚合物P(AMPS-AM-DMAMNVP)的制备及降滤失性能[J].高分子材料与化学工程, 2011,27(4):147-150.

    GAO Lei,SUN Dejun,XU Jian. Preparation and properties of P(AMPS-AM-DMAM-NVP)as fluid loss reducer[J]. Polymer Materials Science and Engineering, 2011,27(4):147-150.
    [10]
    武玉民,孙德军,吴涛,等. 耐温抗盐降滤失剂AMPS/AM/IA共聚物泥浆性能的研究[J]. 油田化学, 2001,18(2):101-104.

    WU Yumin,SUN Dejun,WU Tao,et al. Study on mud properties of amps/am/ia terpolymer as temperature resistant and salt tolerant filtrate reducer[J].Oilfield Chemistry,2001,18(2):101-104.
    [11]
    黄维安,邱正松,曹杰,等. 钻井液用超高温抗盐聚合物降滤失剂的研制与评价[J]. 油田化学,2012,29(2):133-137.

    HUANG Weian,QIU Zhengsong,CAO Jie,et al. Development and evoluation of anti ultra-high temperature and salt tolerant polymeric filtrate loss reduce.[J].Oilfield Chemistry,2012,29(2):133-137.
    [12]
    王中华.P(AMPS-DMAM)共聚物钻井液降滤失剂的合成[J]. 精细与专用化学品,2010,18(7):25-28.

    WANG Zhonghua. Synthesis of the P(AMPS一DMAM) copolymer filtration reducer for drilling fluid[J]. Fine and Specialty Chemicals,2010,18(7):25-28.
    [13]
    姚如钢,蒋官澄,李威,等. 耐温抗盐降滤失剂P (AA-AMPS-AM)/nano-SiO2的合成及性能[J]. 石油化工,2013,42(4):419-424.

    YAO Rugang,JIANG Guancheng,LI Wei,et al. Synthesis and properties of P(AA-AMPS-AM)/nano-SiO2 as fltrate reducer with heat resistance and salt tolerance[J]. Petrochemical Technology,2013,42(4):419-424.
    [14]
    谢建宇,张滨,王旭,等.AA/MA/AMPS共聚物钻井液降黏剂性能评价[J]. 精细石油化工进展,2009:1-7. XIE Jianyu,ZHANG Bin,WANG Xu,et al. Properties of AA/AMPS/DMDAAC copolymer as viscosity reducer for drilling fluids[J]. Andvance in fine Petrochemicals, 2009:1

    -7.
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