Volume 33 Issue 3
May  2016
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GUO Jianhua, MA Wenying, LIU Xiaoyan, DU Mingjun, LI Baohui, ZHONG Ling. Ploya mine Shale Inhibitor Content Measurement and Determination of Optimum Dosage[J]. DRILLING FLUID & COMPLETION FLUID, 2016, 33(3): 35-40. doi: 10.3969/j.issn.1001-5620.2016.03.007
Citation: GUO Jianhua, MA Wenying, LIU Xiaoyan, DU Mingjun, LI Baohui, ZHONG Ling. Ploya mine Shale Inhibitor Content Measurement and Determination of Optimum Dosage[J]. DRILLING FLUID & COMPLETION FLUID, 2016, 33(3): 35-40. doi: 10.3969/j.issn.1001-5620.2016.03.007
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Ploya mine Shale Inhibitor Content Measurement and Determination of Optimum Dosage

doi: 10.3969/j.issn.1001-5620.2016.03.007
  • 1.

    Research Center of Engineering Technology, Zhongyuan Engineering Company, Puyang, Henan 457001

  • 2. No. 2 Drilling Department of Zhongyuan Engineering Company, Puyang, Henan 457001

  • Received Date: 2016-01-05
  • Publish Date: 2016-05-31
    Abstract
  • As a high performance shale inhibitor, polyamine has found a wide application in drilling with water base drilling fluids. Studies on polyamine were primarily focused on the inhibitive capacity and field application, and no technical specifications of polyamine have been established. A method of measuring the content of polyamine is discussed in this paper. Using the "sodium tetraphenylborate method", the content of a free polyamine, FYZ-1, was measured. The measuring method has been determined through the optimization of the testing conditions, such as indicators, precipitation conditions, titration conditions, pH values, etc. The effect of drill cuttings on the content of polyamine has also been studied. It has been founded in laboratory experiments that the quantities of the adsorbed polyamine on carbonaceous shale, hydratable shale, brittle shale and sandstone are decreasing in that order. This finding can be used to determine the concentrations of polyamine in drilling fluids in field operations.

     

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