Volume 32 Issue 6
Nov.  2015
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SUN Zhongfu, WANG Weidong, LI Xiaodi, SUN Zening, GU Tiantian, LI Guiqing, CHEN Zhe, XU Jiafang. Study on Organophilic Clay for Bio-Diesel Oil Base Drilling Fluid[J]. DRILLING FLUID & COMPLETION FLUID, 2015, 32(6): 11-13. doi: 10.3969/j.issn.1001-5620.2015.06.003
Citation: SUN Zhongfu, WANG Weidong, LI Xiaodi, SUN Zening, GU Tiantian, LI Guiqing, CHEN Zhe, XU Jiafang. Study on Organophilic Clay for Bio-Diesel Oil Base Drilling Fluid[J]. DRILLING FLUID & COMPLETION FLUID, 2015, 32(6): 11-13. doi: 10.3969/j.issn.1001-5620.2015.06.003

Study on Organophilic Clay for Bio-Diesel Oil Base Drilling Fluid

doi: 10.3969/j.issn.1001-5620.2015.06.003
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  • Corresponding author: 徐加放,电话(0532)86981190/18678986873
  • Received Date: 2015-06-30
  • Publish Date: 2015-11-30
  • Organophilic clays commonly available for use in white oil and diesel oil do not disperse well in bio-diesel oils which have different molecular structures than those of the white oils and common diesel oils.JHA, an organophilic clay, was recently developed through laboratory study.The base clay selected for the study is the Xiazijie Na-bentonite, and four kinds of organic intercalating agents(ESDS, SSDS, LSDS, and BSDS) were tried in the study to replace the interchangeable cations in between the crystal layers of clays.The ratio of the concentration of clay slurry to that of the intercalating agents is 3:1.JHA has colloidal rate of 98%.To make JHA, the optimum temperature for the reaction should be kept at 70℃, the time for the reaction is 1h, and the selected intercalating agent is ESDS.A mud made with 3.0% JHA in bio-diesel has yield point of about 5 Pa, API filter loss of 21 mL, and remains stable at 180℃.Characterization of JHA with XRD and FTIR shows that the c-spacing of JHA is remarkably increased, and symmetric and asymmetric stretching vibration peaks of-CH2-are observed, indicating that the intercalation agent has been successfully inserted into the crystal layers of bentonite.

     

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