Volume 39 Issue 2
Jun.  2022
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YANG Lili, LIU Hanqing, AO Tian, et al.Study and application of dispersion polymerization in preparing PAM filter loss reducer[J]. Drilling Fluid & Completion Fluid，2022, 39（2）：158-163 doi: 10.12358/j.issn.1001-5620.2022.02.005
Citation: YANG Lili, LIU Hanqing, AO Tian, et al.Study and application of dispersion polymerization in preparing PAM filter loss reducer[J]. Drilling Fluid & Completion Fluid，2022, 39（2）：158-163 doi: 10.12358/j.issn.1001-5620.2022.02.005
shu

Study and Application of Dispersion Polymerization in Preparing PAM Filter Loss Reducer

doi: 10.12358/j.issn.1001-5620.2022.02.005

  • MOE Key Laboratory of Petroleum Engineering, China University of Petroleum （Beijing）, Beijing 102249

  • Received Date: 2021-09-29
  • Accepted Date: 2021-08-29
  • Rev Recd Date: 2021-11-10
  • Publish Date: 2022-06-23
    Abstract
  • A microsphere polyacrylamide (PAM) filter loss reducer FA-25 has been developed with acrylamide monomer through dispersion polymerization. The filtration control performance of FA-25 and other PAMs made through aqueous polymerization and inverse emulsion polymerization was compared. The dispersion polymerization is nontoxic and environmentally friendly, and the product does not need any post-treatment. The product FA-25 was characterized through TEM analysis, TG analysis, particle size analysis and molecular weight analysis through gel chromatography. It was proved that the particles of FA-25 are in a shape of sphere, with particle sizes between 40 nm and 200 nm. The molecular weight of FA-25 is 104,928, and the initial thermal decomposition temperature is 200 ℃. A bentonite slurry treated with 1% FA-25 had its API filtration rate reduced to 13.8 mL, this proves that FA-25 has filtration control performance better than the PAMs made through water solution polymerization and inverse emulsion polymerization. FA-25 functions normally at temperatures up to 200 ℃. Good performance of FA-25 renders it good application prospect.

     

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