压差激活密封剂

郭丽梅; 肖淼; 刘举祥

doi:10.3969/j.issn.1001-5620.2015.01.017

压差激活密封剂

doi: 10.3969/j.issn.1001-5620.2015.01.017

1.
天津科技大学材料科学与化学工程学院, 天津
2. 兰德伟业科技集团有限公司, 北京

基金项目: 国家重大专项"大型油气田及煤层气开发"(2011ZX05013)。

详细信息

作者简介:
郭丽梅,教授,1961年生,现从事油田化学品及精细化学品研究。地址:天津经济技术开发区第十三大街29号天津科技大学6号楼529室;邮政编码300457;电话13920929095;E-mail:glmei@tust.edu.cn。

中图分类号: TE257.12
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出版历程
- 收稿日期: 2014-12-10
- 刊出日期: 2015-01-30

Pressure Activated Sealant

Room 529 of 6th Building, Tianjin University of Science and Technology, No.29, Thirteenth Street, Tianjin Economic and Technological Development Area, Tianjin 300457, china

摘要

摘要: 针对油气井的管件在生产过程中易出现损坏泄露,优选了胶乳、激活剂、终止剂、稳定剂,复配出一种模拟人体创伤流血自身修复的压差激活密封剂。该密封剂的主剂为丁腈胶乳,激活剂为CH₃COONa、MgSO₄和NaCl,终止剂为Gemini1231及Gemini1631,稳定剂为钠基膨润土。研究表明,该密封剂只在出现压差的泄漏点凝固,在其他情况下保持流动状态;使用温度为-20~120℃;密封剂粒度在0~1000μm范围可控,甚至更大。采用φ139.7 mm油管对丝扣进行破坏模拟泄漏,结果显示,泄露速度为600 mL/min时,采用压差激活密封剂停留60 s成功修复,修复后体系在水压为40 MPa和氮气压力为35 MPa时的密封效果符合行业标准。
- 密封剂 /
- 油气井 /
- 压差激活
Abstract: A pressure activated sealant was developed to overcome leaking of oil well pipework. The sealant was formulated with butyronitrile latex as base additive, CH₃COONa, MgSO₄ and NaCl as activators, Gemini1231 and Gemini1631 as terminators and sodium montmorillonite as stabilizer. Laboratory study showed that this sealant only became coagulated at leaking sites where there were differential pressures, otherwise maintained in mobile state. The sealant worked at temperatures between -20℃ and 120℃ and had particle sizes between 0 μm and 1,000 μm, or bigger. In a simulation test with 139.7 mm tubing in which the thread was damaged, when leaking rate was 600 mL/min, the leaking was stopped after applying the sealant and waiting for 60 s. After reparation, no leaking was found for the tubing under 40 MPa of water pressure and 35 MPa of nitrogen gas pressure, satisfying the requirement of industrial standard.
- Sealant /
- Oil and gas well /
- Pressure activate

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参考文献(8)

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