Research Progress, Current Situation Analysis and Development Suggestions of Drilling Fluid Treatment Agents in China
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摘要: 为了解我国在钻井液处理剂取得的新进展，从生物质材料改性产物、合成聚合物材料、缩合化反应产物，以及工业副产和生活废料改性产物等方面，就国内近期钻井液处理剂研制及应用情况进行了综述：生物质改性材料主要用于降滤失剂，以淀粉、纤维素、木质素和腐殖酸为主，且以淀粉居多；合成聚合物材料以用于降滤失剂、增黏剂、包被剂和降黏剂的水溶性聚合物材料研究最多，并围绕提高耐温抗盐和抗高价离子能力，在引入NVP、DMAM等水解稳定性好的单体共聚物方面开展了大量研究，用于封堵和降滤失剂的水不溶性材料也有了一些研究；缩合反应产物集中在用于油基钻井液乳化剂、增黏剂等，以及水基钻井液润滑剂的酯化和酰胺化等缩合反应产物研究；利用工业副产和生活废料制备钻井液处理剂也开展了一些研究。尽管处理剂研究总数量很多，也取得了较好效果，但研究的创新性、深度和覆盖面还不够，因设计思路、合成手段与评价方法的局限性，能够满足现场复杂条件下钻井液性能维护的需要或生命力强的处理剂相对较少，还存在相似或低水平重复研究现象。结合实践，处理剂研究要朝着打破传统思路，突破传统机理，围绕简化钻井液组分、降低钻井液费用、完善钻井液功能、提高钻井液质量和绿色化发展目标，强化生物质资源开发利用，创新合成方法和工艺，开发综合性能好的低成本、高质量、长效多功能材料。Abstract: To understand the new achievements of drilling fluid additives in China, this article reviews the recent development and application of drilling fluid additives, based on modified biomass materials, synthetic polymers, condensation reaction products, modified industrial by-products, and domestic waste modification products. Modified biomass materials, containing starch, cellulose, lignin, and humic acid, are mainly used for fluid loss reducers, and starch is the most common one; the most studied synthetic polymer materials are water-soluble polymers for fluid loss reducers, viscosity enhancers, encapsulating agents, and viscosity reducers. There are also some studies on water-insoluble materials used for plugging and fluid loss reducers. Monomers with good hydrolytic stability such as NVP as well as DMAM are used to enhance temperature-resistant, salt-resistant, and high valent ion-resistant ability. Condensation reaction products focus on emulsifiers and viscosity enhancers of oil-based drilling fluid, and esterification and amidation reaction of lubricants in water-based drilling fluid as well. Some research has also been conducted on the preparation of drilling fluid treatment agents using industrial by-products and household waste. Although there has already been a large number of research on drilling fluid additives, the research is still not innovative, in-depth, and comprehensive enough. Due to the limitations of molecular design, synthetic means, and evaluation methods, there are relatively few drilling fluid additives that can meet the needs of complex fields on site.There is still a phenomenon of similar or low-level repetitive research. Combining with practice. The research on treatment agents should aim to break through traditional thinking and mechanisms. Around the goals of simplifying drilling fluid components, reducing drilling fluid costs, improving drilling fluid functions, enhancing drilling fluid quality, and promoting green development. Strengthen the development and utilization of biomass resources, innovate synthesis methods and processes, and develop low-cost, high-quality, and long-term multifunctional materials with good comprehensive performance.
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表 1 分别加入悬挂基处理剂与传统处理剂钻井液老化后性能对比
t200℃老化/h 引入悬挂基处理剂(相对分子质量10.8×104) P(AM-AA-AMPS)聚合物（相对分子质量约100×104） PV/mPa·s FAPI/mL FHTHP/mL 备注 PV/mPa·s FAPI/mL FHTHP/mL 备注 16 83 0.2 6.8 上下均匀，流动性好 — 0.1 6.2 稠化 32 109 0.4 8.6 上下均匀，流动性好 — 0.4 8.6 底部有沉降 48 92 0.4 10.8 上下均匀，流动性好 — 0.2 10.0 底部有沉降 56 125 0.6 73.6 沉降 112 74 0.1 6.5 上下均匀，流动性好 128 65 0.1 7.8 上下均匀，流动性好 注：①高温高压滤失量测试温度为180℃，对比聚合物是P(AM-AA-AMPS)；②实验浆配方：4%膨润土+5%SMC+4.5%聚合物+1.0%NaOH+30%NaCl+重晶石，密度为2.1 g/cm3；③“—”钻井液太稠，超黏度计量程。 
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